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"Diff Con 1" Differential Conductance
Warning: This is a work in progress. Take everything with a grain of salt!
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Downloads
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I am curious who uses what. Are these webpages a waste of time, or are they any help to others? Are the circuits, software and utilities appearing in other labs? Please send your comments or suggestions or what you have used (or not) or schematics of your version or pictures or anything! Email me, or be creative and send a postcard! I want to hear from the vacuum! |
Links
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NOTICE: This webpage and associated files are provided for reference only. This is not a kit site! It is a collection of my work here at the University of Toronto in the Physics department. If you are considering using any schematics, designs, or anything else from here then be warned that you had better know something of what you are about to do. No design is guaranteed in any way, including workable schematic, board layout, HDL code, embedded software, user software, component selection, documentation, webpages, or anything. All that said, if it says here it works then for me it worked. To make the project work may have involved undocumented additions, changes, deletions, tweaks, tunings, alterations, modifications, adjustments, waving of a wand while wearing a pointy black hat, appeals to electron deities and just plain doing whatever it takes to make the project work. |
Started 2013 May for Parisa Zareapo in Ken Burch's lab. This apparatus measures static and dynamic (AKA differential) resistance (or conductance) of junctions with two materials, where one, both or neither may be superconducting. A sub-Volt DC voltage with a small AF AC excitation is applied to a 4-wire sample in a cryostat. The AC and DC voltages and currents are measured and sent back to the host (the controlling computer). The sample is galvanically isolated from the cryostat and any ground or earth.
A DAC generates the required static voltage. An on-board oscillator generates the AC component, the amplitude of which is controlled by a digital pot. The DC and AC are summed in an opamp with current boosting. This opamp output is attenuated with selectable low tempco resistors. Four measurements by four ADCs are made: voltage and current of both the DC and AC components. AC measurements are phase locked to the AC peak and minimum. Although the absolute amplitude of the AC voltage and current at its peak and minimum should be the same, both are taken to reduce errors. Similarly, the AC frequency, which is in the audio range, can be varied to reduce reactive effects of the sample, the cabling and this unit.
Voltage across the sample is with four connections: two current drives and two measurement, also known as Kelvin measurement. The four connections are BNC. The BNC shields are connected to the board through 100 Ohms each. One shield must be connected to an earth ground. Empirically, experiment with grounds on one or more shields for lowest noise. This cannot be calculated, it must be tested with trial and error.
Two sets of four BNCs are provided. They are identical. While one set may be the sample under test, the other can be a standard resistor used for calibration. Select the active set with the front panel switch.
Left - Drive Level | Right - Current Sense | ||||||
# | Normalized | Voltage | Resistance | # | DC Resistance | AC Resistance | |
1 | out | out | out | 1 | 1 | 1 | |
2 | 1 | 4.095V | 10 | 2 | 10 | 10 | |
3 | 1 | 4.095 | 100 | 3 | 100 | 100 | |
4 | 0.20325 | 0.83232 | 79.7 | 4 | 1K | 1K | |
5 | 0.090909 | 0.37227 | 9.0909 | 5 | 10K | 10K | |
6 | 0.020619 | 0.084433 | 9.7938 | 6 | 100K | 90.9K | |
7 | 0.099010 | 0.040545 | 0.9901 | 7 | 1M | 500K | |
8 | 0.002101 | 0.008603 | 0.9979 | 8 | out | out | |
9 | out | out | out | 9 | out | out | |
10 | out | out | out | 10 | out | out |
Gains, Resolution and Measurement
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Measurement | Settings | per LSB | Full Scale | Comments |
DC Voltage | 10.167µV | ±333.13mV | ||
DC Current | Depends on current sense setting | 11.36µV | ±372.3mV | Voltage across current sense resistor |
AC Voltage | Gain X1 | 62.485µV | ±2.048V | Do not use, provided for continuity only |
Gain X3 | 20.828µV | ±682.50mV | Only useful ±200-300mV | |
Gain X10 | 6.249µV | ±204.75mV | ||
Gain X30 | 2.089µV | ±68.250mV | ||
Gain X100 | 0.6249µV | ±20.475mV | ||
Gain X300 | 0.2083µV | ±6.8250mV | ||
AC Current
(voltage across current sense resistor) |
Gain X1 | 62.485µV | ±2.048V | Do not use, provided for continuity only |
Gain X3 | 20.828µV | ±682.50mV | Only useful ±200-300mV | |
Gain X10 | 6.249µV | ±204.75mV | e.g. Current sense 2 (10^3 or 1K) = 6.25nA/LSB and 205µA FS | |
Gain X30 | 2.089µV | ±68.250mV | ||
Gain X100 | 0.6249µV | ±20.475mV | ||
Gain X300 | 0.2083µV | ±6.8250mV |
Parameter | Min | Typ | Max | Conditions and Comments |
Drive Source | ||||
Load resistance | 1 Ohm | 1M Ohm | ||
DC voltage | -300mV | +300mV | ||
DC current | -300mA | +300mA | Fused at 400mA | |
DC resolution | 1mV | |||
AC voltage | 0uV | 5mV | RMS | |
AC current | - | 5mA | RMS, depending on load | |
AC frequency | 25Hz | 1KHz | SINAD <1% | |
ADCs | ||||
Resolution | 16 | Bits | ||
ENOB | 14.5 | Measured, estimated |
Sorry, no more chance for asking direct questions, queries, broken links, problems, flak, slings, arrows, kudos, criticism, comments, brickbats, corrections or suggestions. |
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